NMR Spectroscopy Core Facility

 
The Nuclear Magnetic Resonance (NMR) facility at the ICCBS is a Core Research Support Unit. The facility serves mostly undergraduate, graduate, doctoral, and post-doctoral researchers, in the field of Chemistry, Chemical, and Biomolecular Engineering Departments from all over the country.

The facility presently operates thirteen superconducting NMR spectrometers (Bruker) of varying capabilities. The 800 MHz Bruker Ascend NMR spectrometer is the newest addition to the NMR facility, of the ICCBS. The equipment is featured with an Avance III HD console (5 RF channels, 2 receivers), equipped with a TCI (1H/13C/15N/31P/2H) CryoProbe, which is a H-optimized triple resonance NMR 'inverse' probe, and also a RT probe. Four instruments (one 800 MHz, two 600 MHz, and one 500 MHz) are equipped with cryogenically cooled probes. Two of our 400 MHz are equipped with multinuclear probe to detect a wide range of elements.  Recently, SampleCase™ is fitted to 600 MHz spectrometer that provides easy, safe and convenient access to fully-fledged NMR automation. It can accommodate 24 samples. The NMR instruments are accessible to trained users 24 hours/day, year-round.

The facility also serve corporate and industrial clients, and offer a full range of NMR spectroscopy service options from routine 1D H spectra acquisition and interpretation to complex 2D NMR analysis for the verification of their products as well as contaminants. The facility provides on request training to the researcher, from Pakistan, as well as to the researchers of other developing countries to enable users to independently operate the NMR spectrometers.
 
  

 
NMR SPECTROMETERS
 
Bruker AVANCE-III-HD 800 MHz
Available Probes

5 mm CPTCI 1H, 13C, 15N 0.5Z-GRD
5mm PATXI 1H, 13C, 15N 0.5Z-GRD
Available channels
Four channels (1H, 13C, 15N and 31P)

 
Bruker AVANCE NEO 600 MHz LC NMR 
Available Probes

5 mm CPTCI 1H, 13C, 15N Z-GRD
5mm TXI 1H, 13C, 15N Z-GRD
Available channels
Three channels (1H, 13C and 15N) 

 

 
Bruker AVANCE NEO 600 MHz
Available Probes
5
 mm CPTCI 1H, 13C, 15N Z-GRD
5mm BBI 1H, 13C, 15N Z-GRD
Available channels
Three channels (1H, 13C and 15N) + Deuterium Decoupling
Fitted with Sample case

 
Bruker AVANCE NEO 500 MHz
Available Probes
5 mm CPDUL 1H, 13C Z-GRD
Available channels
Two channels (1H and 13C)
 
Bruker AVANCE NEO 500 MHz
 
Available Probes
5 mm TXI 1H, 13C/ D-BB Z-GRD
Available channels
Three channels 1H, 13C, and 15N
 
Bruker AVANCE NEO 500 MHz    
Available Probes
5 mm BBI 1H, 13C / D-BB Z-GRD
Available channels
Two channels (1H and 13C)
 
Bruker AVANCE NEO 400 MHz
Available Probes
5 mm DUL 1H,13C/ D  Z-GRD
5 mm PABBO 1H, 13C/ D-BB Z-GRD (Smart Probe)
5 mm BBO 1H,13C/ D  Z-GRD
Available channels
Two channels (1H and X)

 
Bruker AVANCE NEO 400 MHz
Available Probes

5 mm PABBO 1H, 13C/ D-BB Z-GRD (Smart Probe)
Available channels
Two channels (1H and X Nuclei)
 
Bruker AVANCE-III 400 MHz
Available Probes

5 mm PABBO 1H, 13C/ D-BB Z-GRD (Smart Probe)
Available channels
Two channels (1H and X Nuclei)

 
Bruker AV-III- 300 MHz
Available Probes
5 mm BBO BB 1H, 13C/ D Z-GRD
Available channels
Two channels (1H and 13C)
 
Bruker AVANCE NEO 300 MHz
Available Probes
5 mm DUL 1H, 13C/ D Z-GRD
Available channels
Two channels (1H and 13C)
 
Bruker AV 300 MHz
Available Probes

5 mm BBO BB 1H, 13C / D Z-GRD
Available channels
Two channels (1H and 13C)